Rapid reactive synthesis of TiAl3 intermetallics by ...
Al mixture powders were evenly wet-mixed in a planetary ball mill at 450 rpm/min for 4 h. Ethyl alcohol was used as the milling medium to avoid oxidation and agglomeration. Then the cylindrical green compacts were prepared in a stainless steel mold with 16 mm in diameter and 2–3 mm in height, the uniaxial pressure was set to 300 MPa for 2 min.
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